[3dem] Tip-side leak on Gatan 626
Buecker, Robert
robert.buecker at mpsd.mpg.de
Fri Jun 22 07:40:03 PDT 2018
Dear List,
we are having a problem with an old (1984) Philips-type Gatan 626 cryo-transfer holder which we are using in a Tecnai F20. After it had caused venting of the column several times while inserting or rectracting, we found using a pump station that it must have a leak on the tip-sided seal between column and dewar vacuum (the base pressure in the pump station did not fall beyond 2e-5 mbar, and venting the dewar while inserted raised it to 1.5e-3).
Did any of you ever have that problem, and if so, do you know of some way to fix it without sending it in for service?
Best regards,
Robert
--
dr. robert bücker
max planck institute for the structure and dynamics of matter
atomically resolved dynamics department
desy bldg. 99 (cfel)
luruper chaussee 149
22761 hamburg, germany
tel. +49 40 8998-6278 / -86043
mob. +49 157 70210628
robert.buecker at mpsd.mpg.de
http://www.mpsd.mpg.de/68786/Femtosecond_Diffraction
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